COURSE SYLLABUS

STRUCTURE IDENTIFICATION IN ORGANIC CHEMISTRY

1	Course Title:	STRUCTURE IDENTIFICATION IN ORGANIC CHEMISTRY
2	Course Code:	KIM6042
3	Type of Course:	Optional
4	Level of Course:	Third Cycle
5	Year of Study:	1
6	Semester:	2
7	ECTS Credits Allocated:	5
8	Theoretical (hour/week):	3
9	Practice (hour/week) :	0
10	Laboratory (hour/week) :	0
11	Prerequisites:
12	Recommended optional programme components:	None
13	Language:	Turkish
14	Mode of Delivery:	Face to face
15	Course Coordinator:	Prof. Dr. NECDET COŞKUN
16	Course Lecturers:	-
17	Contactinformation of the Course Coordinator:	coskun@uludag.edu.tr +90 224 29 41 725 Uludağ Üniversitesi, Fen-Edebiyat Fakültesi, Kimya Bölümü, 16059 Görükle / BURSA, TÜRKİYE
18	Website:
19	Objective of the Course:	The objective of the course is teach the basic principles of spectroscopic techniques (IR, H-NMR, C NMR, MS, UV) and interpreting spectrum of organic compounds.
20	Contribution of the Course to Professional Development

Learning Outcomes:

1	IR, 1H-NMR and 13C-NMR, UV-VIS spectrophotometer, and mass spectrometry, recognize the basic components of devices;
2	IR, 1H-NMR and 13C-NMR, UV-VIS spectroscopic techniques, understanding detailed theory of mass spectrometry technique;
3	To improve ability to receive spectrum and sample preparation for each technique mentioned above;
4	To interpret correctly the spectra of organic compounds taken by IR, 1H-NMR 13C-NMR, UV-VIS and mass spectrometry techniques;
5	Identification of the structures of organic compounds by using the spectroscopic and spectrometric techniques;

22	Course Content:

Week	Theoretical	Practical
1	The theory of IR spectroscopy and sample preparation techniques The theory of IR spectroscopy Sample preparation techniques for the get of the spectrum
2	IR spectrum interpretations Characteristic group frequencies Spectrum interpretation
3	The of theory 1H-NMR and 13C-NMR spectroscopy The theory of 1H-NMR spectroscopy The theory of 13C-NMR spectroscopy
4	Sample preparation for NMR Sample preparation techniques, and techniques for the getting of NMR spectra
5	Interpretation of NMR spectra interpretation the 1H-NMR and 13C-NMR spectras of the organic compounds
6	Factors affecting chemical shift, spin-spin coupling Chemical shift The factors determining the chemical shifts diamagnetic anisotropy Spin-spin interactions and the factors affecting
7	Interpretation of first-order spectra Interpretation of the first order 1H-NMR and 13C-NMR spectra of different classes of organic compounds
8	Two-dimensional (2D)-NMR techniques 2D-spectroscopy and theory COSY, HETCOR and interpretation of the spectra
9	The basic principles of UV-VIS spectroscopy The theory of the method and electronic excitations The technique to get pectrum Spectrum interpretation, the effect of conjugation
10	Mass spectrometry The theory of mass spectrometry Ionization techniques The basic components of the device Sample preparation and getting of the spectrum
11	Determination of molecular formula, molecular ion peaks Determination of molecular weights Determination of molecular formula Tthe molecular ion peak and its determination
12	Mass spectra interpretation Mass spectrum interpretation and using the technique for structure elucidation Structural analysis and fragmentations of the different classes of organic compound
13	The use of these techniques together for the structure elucidation The interpretation of the structures of known or unknown organic compounds by using these techniques together
14	The use of these techniques together for the structure elucidation The interpretation of the structures of known or unknown organic compounds by using these techniques together

23	Textbooks, References and/or Other Materials:	[1] Metin Balcı, “Nükleer manyetik rezonans spektroskopisi’’, Ankara, 2011 [2] D.L.Pavia, G.M.Lampman, G.S.Kriz, “Introduction to Spectroscopy’’, Brooks Cole, 2000 [3] T.D.W.Claridge “HIGH-RESOLUTION NMR TECHNIQUES IN ORGANIC CHEMISTRY’’, Elsevier Science,2011
24	Assesment

TERM LEARNING ACTIVITIES	NUMBER	PERCENT
Midterm Exam	0	0
Quiz	0	0
Homeworks, Performances	1	50
Final Exam	1	50
Total	2	100
Contribution of Term (Year) Learning Activities to Success Grade		50
Contribution of Final Exam to Success Grade		50
Total		100
Measurement and Evaluation Techniques Used in the Course
Information

ECTS / WORK LOAD TABLE

Activites	NUMBER	TIME [Hour]	Total WorkLoad [Hour]
Theoretical	14	2	28
Practicals/Labs	14	2	28
Self Study and Preparation	14	1	14
Homeworks, Performances	1	40	40
Projects	0	0	0
Field Studies	0	0	0
Midtermexams	0	0	0
Others	0	0	0
Final Exams	1	72	72
Total WorkLoad			182
Total workload/ 30 hr			6,07
ECTS Credit of the Course			6

CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS

	PQ2	PQ3	PQ4	PQ5	PQ7
LO1	5	5	5	4	4
LO2	5	5	5	4	4
LO3	5	5	5	4	4
LO4	5	5	5	4	4
LO5	5	5	5	4	4

LO: Learning Objectives

PQ: Program Qualifications

Contribution Level:

1 Very Low

2 Low

3 Medium

4 High

5 Very High