COURSE SYLLABUS

COMBINED ANALYTICAL TECHNIQUES IN ELEMENTARY GENERATION

1	Course Title:	COMBINED ANALYTICAL TECHNIQUES IN ELEMENTARY GENERATION
2	Course Code:	KIM4066
3	Type of Course:	Optional
4	Level of Course:	First Cycle
5	Year of Study:	4
6	Semester:	8
7	ECTS Credits Allocated:	5
8	Theoretical (hour/week):	3
9	Practice (hour/week) :	0
10	Laboratory (hour/week) :	0
11	Prerequisites:	To take the optional course of "Inductively Coupled Plasma (ICP) Analysis Techniques"
12	Recommended optional programme components:	None
13	Language:	Turkish
14	Mode of Delivery:	Face to face
15	Course Coordinator:	Doç. Dr. ÜMRAN SEVEN ERDEMİR
16	Course Lecturers:	Prof. Dr. Belgin İZGİ
17	Contactinformation of the Course Coordinator:	Doç. Dr. Ümran SEVEN ERDEMİR Bursa Uludağ Üniversitesi Fen-Edebiyat Fakültesi Kimya Bölümü 16059 Görükle-Nilüfer/Bursa Tel: 0224 29 42943 e-posta: useven@uludag.edu.tr
18	Website:
19	Objective of the Course:	The aim of the course is to gain knowledge to chemistry students in elemental speciation and inductively coupled plasma (ICP) technique. Students will be learn the importance of elemental speciation analysis in food or environmental samples. Coupled analytical techniques combined with different separation methods in which ICP-MS is used as a detector will be introduced to ensure that students have sufficient knowledge about the devices with different combinations, hardware, software, operating principles, measurement methods, interpretation of the outputs. Current studies in elementary speciation analysis will be given as examples from the literature and students will gain sufficient knowledge about the analytical importance of the results.
20	Contribution of the Course to Professional Development	The student will learn the ICP-MS based combined analytical techniques that allow elemental analysis studies based on organic matrix, and will be able to look at total metal analysis in different dimensions in terms of toxicity and bioavailability.

Learning Outcomes:

1	Learns the importance of elemental speciation.;
2	Learns the technological importance and differences of applications of coupled analytical techniques in which the ICP-MS device is used as a detector.;
3	Gains knowledge about analytical approaches to coupled analytical techniques through current examples of elemental speciation from the literature. ;
4	Gains the ability of the transfer of the current knowledge on a given subject by presentation.;
5	Uses foreign language knowledge at a level to follow the current literature within the context of coupled analytical techniques in elementary speciation.;

22	Course Content:

Week	Theoretical	Practical
1	Description of coupled analytical techniques and needs for their use
2	ICP-MS as a detector in coupled analytical techniques
3	Introduction to current ICP-MS coupled techniques and current applications: new approaches to total metal determination, speciation analysis and requirements
4	Comparison of collision / reaction cell (CC-ICP-MS / DRC-ICP-MS) with standard mode ICP-MS
5	GC-ICP-MS as a coupled analytical technique, basic principles
6	GC-ICP-MS, device components / application areas
7	HPLC/LC-ICP-MS as a coupled analytical technique, basic principles
8	HPLC/LC-ICP-MS, device components / application areas
9	Application areas of HPLC-HG-ICP-MS as a coupled analytical technique
10	CE-ICP-MS as a coupled analytical technique, basic principles
11	CE-ICP-MS, device components / application areas
12	LA-ICP-MS as a coupled analytical technique, basic principles
13	Submission of homework + LA-ICP-MS, device components / application areas
14	Current trends in quantitative analysis of tin, lead, mercury, chromium, selenium, arsenic species using coupled ICP-MS techniques

23	Textbooks, References and/or Other Materials:	• Hyphenated Techniques in Speciation Analysis, Joanna Szpunar, Ryszard Lobinski, Ed. Roger M. Smith, Royal Society of Chemistry, 2003 • Analytical Atomic Spectrometry with Flames and Plasmas, 2nd, Completely Revised and Enlarged Edition, José A. C. Broekaert, Wiley, ISBN: 978-3-527-31282-5 July 2005. • Skoog-Holler-Nieman, Enstrumental Analiz (çeviri), Bilim Yayıncılık, 1998
24	Assesment

TERM LEARNING ACTIVITIES	NUMBER	PERCENT
Midterm Exam	1	30
Quiz	0	0
Homeworks, Performances	1	10
Final Exam	1	60
Total	3	100
Contribution of Term (Year) Learning Activities to Success Grade		40
Contribution of Final Exam to Success Grade		60
Total		100
Measurement and Evaluation Techniques Used in the Course	Traditional and new complementary approaches will be used together in measurement. Traditional methods (80% effective): 1. Classic written exam (2 exams, mid-term and final) 2. Quizzes (4 exams during the semester) Complementary methods (20% effective): 1. Performance evaluation by assigning research homework and making oral presentations 2. Observation / self-assessment according to participation with answering questions asked during the lesson The evaluation will be made according to the scores specified in Bursa Uludağ University Undergraduate Education and Training Regulations for classes with less than 20 students or by relative evaluation system for classes more than 20.
Information

ECTS / WORK LOAD TABLE

Activites	NUMBER	TIME [Hour]	Total WorkLoad [Hour]
Theoretical	14	3	42
Practicals/Labs	0	0	0
Self Study and Preparation	14	3	42
Homeworks, Performances	1	10	10
Projects	0	0	0
Field Studies	0	0	0
Midtermexams	1	20	20
Others	0	0	0
Final Exams	1	40	40
Total WorkLoad			154
Total workload/ 30 hr			5,13
ECTS Credit of the Course			5

CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS

	PQ1	PQ2	PQ3	PQ4	PQ5	PQ6	PQ7	PQ8	PQ9	PQ10	PQ11	PQ12	PQ13
LO1	1	1	1	3	3	1	2	1	1	1	1	3	3
LO2	1	1	1	4	3	1	2	1	2	1	2	3	3
LO3	1	1	1	3	3	1	2	1	2	1	2	3	3
LO4	1	1	1	1	1	4	4	4	3	4	3	3	3
LO5	1	1	1	1	1	2	2	3	2	4	3	3	3

LO: Learning Objectives

PQ: Program Qualifications

Contribution Level:

1 Very Low

2 Low

3 Medium

4 High

5 Very High