SEPERATION AND PURIFICATION TECHNIQUES IN ORGANIC CHEMISTRY
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Course Title:
SEPERATION AND PURIFICATION TECHNIQUES IN ORGANIC CHEMISTRY
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Course Code:
KIM5029
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Type of Course:
Optional
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Level of Course:
Second Cycle
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Year of Study:
1
6
Semester:
1
7
ECTS Credits Allocated:
6
8
Theoretical (hour/week):
3
9
Practice (hour/week) :
0
10
Laboratory (hour/week) :
0
11
Prerequisites:
None
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Recommended optional programme components:
None
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Language:
Turkish
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Mode of Delivery:
Face to face
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Course Coordinator:
Doç.Dr. NEVİN ARIKAN ÖLMEZ
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Course Lecturers:
Prof.Dr.Mustafa Tavaslı
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Contactinformation of the Course Coordinator:
narikan@uludag.edu.tr Tel: 0 (224) 294 1731 Uludağ Üniversitesi Fen-Edebiyat Fakültesi Kimya Bölümü, Görükle/BURSA 16059
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Website:
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Objective of the Course:
The aim of the course is to provide theoretical and practical skills to master students with laboratory techniques used in organic chemistry.
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Contribution of the Course to Professional Development
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Learning Outcomes:
1
Developing of the knowledge and experience about the isolation of the product after organic synthesis;
2
Increasing of the info and accumulation about organic synthesis;
3
Earning the ability to crack against to problems that could occur in thesis works of the students studied master science in organic chemistry.;
4
Developing the organic chemistry laboratory culture and skill;
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Course Content:
Week
Theoretical
Practical
1
Synthesis of organic compounds
-Planning of the reaction
-Set up of installation
-Reaction completion
2
Filtering techniques
-Classificiation of filtering techniques
-Materials used in filtering techniques
-Applications of filtering techniques
3
Crystallization
-Crystallization steps
-Solvents used in crystallization and selection of the solvent
-Applications of crystallization technique
4
Distillation
-Classification of distillation techniques
-Differents between of the distillation techniques
-Applications of distillation techniques
5
Sublimation and Extraction
-Formation conditions of sublimation
-Samples and applications to the sublimated compounds
-Classification of extraction techniques
-Solvents used in extraction and selection of the solvent
6
Chromatographic techniques
-Column chromatography technique
-Adsorbents and moving phases used in Column chromatography
-Application of column chromatography
7
Chromatographic techniques
-Thin layer chromatography technique
-Adsorbents and moving phases used in thin layer chromatography
-Application of thin layer chromatography
8
Chromatographic techniques
- Paper chromatography theory and techniques
9
Chromatographic techniques
-Theory of Gas chromatography (GC) technique
-Adsorbents and moving phases used in GC
-GC apparatus and applications
10
Chromatographic techniques
-Theory of HPLC technique
-Adsorbents and moving phases used in HPLC
-HPLC apparatus and applications
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Drying
-Drying process and bringing to constant weigh
-Equipments used in drying process
-Applications of drying process
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Determination of physical properties
-Central physical properties of organic compounds
-Variations of the physical properties of organic compounds
-Determination of melting point and the relationship between melting point and purity
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Optical activity
-Description of optical activity
-Which compounds are optical active?
-Chirality and samples to compounds contained chiral carbon
-Enantiomerism and samples to the compounds shown enantiomer property
-Diastereomerism and samples to the compounds shown diastereomer property
-Meso compounds
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Specific angle of rotation
-Description of the specific angle of rotation
-Factors that affect angle of rotation
-Experimental determination of the specific angle of rotation
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Textbooks, References and/or Other Materials:
1) Techniques and experiments for organic chemistry. Addison Ault 2) Organic chemistry microscale laboratory techniques. R. Wooley, D. Shelley, B. Hinshaw 3) Laboratory techniques for organic chemistry.Ralph J. Fessenden, Joan S. Fessenden
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Assesment
TERM LEARNING ACTIVITIES
NUMBER
PERCENT
Midterm Exam
1
40
Quiz
0
0
Homeworks, Performances
0
0
Final Exam
1
60
Total
2
100
Contribution of Term (Year) Learning Activities to Success Grade
40
Contribution of Final Exam to Success Grade
60
Total
100
Measurement and Evaluation Techniques Used in the Course
Information
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ECTS / WORK LOAD TABLE
Activites
NUMBER
TIME [Hour]
Total WorkLoad [Hour]
Theoretical
14
3
42
Practicals/Labs
0
0
0
Self Study and Preparation
14
1
14
Homeworks, Performances
0
0
0
Projects
0
0
0
Field Studies
0
0
0
Midtermexams
1
48
48
Others
0
0
0
Final Exams
1
72
72
Total WorkLoad
176
Total workload/ 30 hr
5,87
ECTS Credit of the Course
6
26
CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS
