COURSE SYLLABUS

ORGANIC CHEMISTRY LABORATORY II

1	Course Title:	ORGANIC CHEMISTRY LABORATORY II
2	Course Code:	KIM2014
3	Type of Course:	Compulsory
4	Level of Course:	First Cycle
5	Year of Study:	2
6	Semester:	4
7	ECTS Credits Allocated:	4
8	Theoretical (hour/week):	0
9	Practice (hour/week) :	0
10	Laboratory (hour/week) :	4
11	Prerequisites:
12	Recommended optional programme components:	None
13	Language:	Turkish
14	Mode of Delivery:	Face to face
15	Course Coordinator:	Prof. Dr. MUSTAFA TAVASLI
16	Course Lecturers:	Prof. Dr. Mustafa TAVASLI Doç. Dr. Nevin ARIKAN ÖLMEZ
17	Contactinformation of the Course Coordinator:	coskun@uludag.edu.tr +90 224 29 41 725 Fen-Edebiyat Fakültesi, Kimya Bölümü, 16059 Görükle, Bursa TÜRKİYE
18	Website:
19	Objective of the Course:	Experimental realization of various reactions learned in Organic Chemistry I and Organic Chemistry II lessons, and synthetic applications of various classes of organic compound by the students
20	Contribution of the Course to Professional Development

Learning Outcomes:

1	Recognition of equipment and glass material which is necessary for the synthesis experiment in organic chemistry lab. Acquiring the ability to establish the relevant reaction apparatus.;
2	Be able to following the reaction, properly termination and isolation of the synthesized product with the appropriate purification method.;
3	Recognize and know the literature of chemistry, survey various computerized literature databases of organic chemistry;
4	Ability to determine the structure of an unknown organic compound given to him in the laboratory, with remembering the functional groups of organic compounds and their reactions with each other;

22	Course Content:

Week	Theoretical	Practical
1		Introduction
2		Fischer esterification reaction Esters and their properties Various methods of preparation of esters preparation of acetate esters of acetic acid with various alcohols catalyzed by H2SO4. Quiz
3		Grignard reaction Organometallic compounds Establishment of the apparatus designed for the Grignard reaction synthesis and characterization of triphenyl methanol with the suitable reaction sequence. Quiz
4		Survey the literature Introduction to the literature of chemistry Introduction of databases related to the organic chemistry Selection of research topics and given to each student.
5		Diels-Alder reaction Introduction of the cycloaddition reactions And the introduction of dienes and dienophiles Mechanism and various examples of Diels-Alder reaction stereochemistry of the reaction Realization of Diels-Alder reaction between the sulpholene (1,3-butadiene source) and maleic anhydride. Quiz
6		Tetrafenilsiklopentadienon synthesis (Week 1) Introduction to Condensation reactions benzoin condensation Thiamine catalyzed benzoin synthesis. Quiz
7		Tetrafenilsiklopentadienon synthesis (Week 2) Conversion of benzoine into benzil with HNO3 Synthesis of tetraphenyl cyclopentadienone compound via the dibenzyl ketone and benzil. Quiz
8		Synthesis of adipic acid from cyclohexanone Oxidation reactions in organic chemistry Oxidation of cyclohexanone to adipic acid in the presence of KMnO4. Quiz
9		Sulfonation of toluene Electrophilic aromatic substitution reactions Sulpohation of toluene with sulfuric acid and synthesis of sodium p-toluenesulfonate. Quiz
10		Problem solving MIDTERM EXAM.
11		Synthesis of butyl bromide Nucleophilic substitution reactions in organic chemistry n-Butyl bromide synthesis from n-butanol with NaBr and H2SO4 . Quiz
12		Organic qualitative analysis (known sample analysis) Fusion of known organic compund with Na and determination its elements, solubility tests, Functional group tests sulphanilic acid Melting point determination, determining the structure of sulphanilic acid by using the Handbooks .
13		Organic qualitative analysis (unknown sample analysis) Fusion of unknown organic compund with Na and determination its elements, solubility tests, Functional group tests sulphanilic acid Melting point determination, determining the structure of unknown organic compound by using the Handbooks .
14		Organic Qualitative Analysis (unknown samples analysis) Completation of trials missing 11 th week to determine the structure of unknown organic compound .

23	Textbooks, References and/or Other Materials:	1) G. Solomons ve C. Fryhle ;(Çev. Ed. G. Okay ve Y. Yıldırır), Organik Kimya; Literatür Yayınları, 2002. 2) Kenneth L. Williamson ; Macroscale and Microscale Organic Experiments,; D.C. Healt and Company, 1989. 3) Brian S. Furniss, Antony J. Hannaford, Peter W.G. Smith, Austin R. Tatchell; Vogel’s Textbook of Practical Organic Chemistry,; Longman Scientific &Technical,; 1989. 4) Ender Erdik, Metin Obalı, Nadire Yüksekışık, Atilla Öktemer, Tarık Pekel, İhsanoğlu; Denel Organic Kimya; A.Ü.F.F Döner Sermaye İşletmesi yayınları, 2000.
24	Assesment

TERM LEARNING ACTIVITIES	NUMBER	PERCENT
Midterm Exam	1	25
Quiz	1	25
Homeworks, Performances	0	0
Final Exam	1	50
Total	3	100
Contribution of Term (Year) Learning Activities to Success Grade		50
Contribution of Final Exam to Success Grade		50
Total		100
Measurement and Evaluation Techniques Used in the Course
Information

ECTS / WORK LOAD TABLE

Activites	NUMBER	TIME [Hour]	Total WorkLoad [Hour]
Theoretical	0	0	0
Practicals/Labs	14	4	56
Self Study and Preparation	14	1	14
Homeworks, Performances	0	0	0
Projects	0	0	0
Field Studies	0	0	0
Midtermexams	1	25	25
Others	0	0	0
Final Exams	1	25	25
Total WorkLoad			120
Total workload/ 30 hr			4
ECTS Credit of the Course			4

CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS

	PQ1	PQ2	PQ3	PQ4	PQ5	PQ6	PQ7	PQ8	PQ10	PQ11
LO1	5	5	5	5	5	5	0	0	0	5
LO2	0	5	5	0	5	5	0	0	0	0
LO3	0	0	0	0	5	0	5	5	4	0
LO4	5	5	5	5	5	0	0	0	0	0

LO: Learning Objectives

PQ: Program Qualifications

Contribution Level:

1 Very Low

2 Low

3 Medium

4 High

5 Very High