Türkçe English Rapor to Course Content
COURSE SYLLABUS
CYCLIC VOLTAMMETRY
1 Course Title: CYCLIC VOLTAMMETRY
2 Course Code: KIM5016
3 Type of Course: Optional
4 Level of Course: Second Cycle
5 Year of Study: 1
6 Semester: 2
7 ECTS Credits Allocated: 6
8 Theoretical (hour/week): 3
9 Practice (hour/week) : 0
10 Laboratory (hour/week) : 0
11 Prerequisites: None
12 Recommended optional programme components: None
13 Language: Turkish
14 Mode of Delivery: Face to face
15 Course Coordinator: Prof. Dr. MEHMET HALUK TÜRKDEMİR
16 Course Lecturers: Yok
17 Contactinformation of the Course Coordinator: Tlf: 2941741
e-mail: hturkdemir@uludag.edu.tr
18 Website:
19 Objective of the Course: This course is planned for to learn of knowledge about cyclic voltammetry basic knowledge and electrochemical characterization of various substances, and especially planned for graduate students from outside of the Electrochemistry.
20 Contribution of the Course to Professional Development
21 Learning Outcomes:
1 To have the basic cyclic voltammetry and knowledge and its intended use.;
2 To know needed items of cyclic voltammetry and knowledge of experimental studies;
3 He can made redox characterization.of new chemicals in aqueous or non-aqueous media;
22 Course Content:
Week Theoretical Practical
1 Cyclic voltammetry definition and usage, basic information of potentiostat
2 Three-electrode cell voltammetry, the components, the electrode-solution interface, double layer structure, junction potential.
3 The working electrodes (WE), variation and selection, selection criteria, GCE and Pt electrode
4 Mercury working electrodes, working surface area
5 Voltammetric reference electrode, types and characteristics
6 Auxiliary electrode and the required properties, IR drop, IR Compensation
7 Supporting electrolyte, specifications, oxygen removal,
8 Establishment of potential screening programs, scanning speed, potential limits, number of cycles
9 Peak potential, peak current and measurements, Randles-Sevcik equation
10 General reminders, description of unifying concepts and Midterm
11 Reversibility, semi-reversibility, irreversibility in cyclic voltammetry curves.
12 Electron transfer mechanisms, gradual electron transfer steps and be monitored on voltammograms
13 Examination of EC, CE, ECE and mechanisms, effects on voltammograms.
14 Cyclic voltammetry in an anhydrous conditions, solvents, supporting electrolyte, reference electrodes, pseudo-reference electrode for non-aqueous solutions.
23 Textbooks, References and/or Other Materials: 1. Techniques and Mechanisms in Electrochemistry, P.A. Christensenand A. Hamnett, Kluwer Acad. Pub.1994
2. Fundamentals of Electrochemistry, V. S. Bagotsky, WILEY 2006
3. Electrochemistry, Principles, Methods, and Applications, C.M.A. Brett, A.M.O. Brett, Oxford 1993
4. Analytical Electrochemistry, J. Wang, WILEY 2001
24 Assesment
TERM LEARNING ACTIVITIES NUMBER PERCENT
Midterm Exam 1 30
Quiz 0 0
Homeworks, Performances 1 10
Final Exam 1 60
Total 3 100
Contribution of Term (Year) Learning Activities to Success Grade 40
Contribution of Final Exam to Success Grade 60
Total 100
Measurement and Evaluation Techniques Used in the Course
Information The weights of the activities can vary within regulations.
25 ECTS / WORK LOAD TABLE
Activites NUMBER TIME [Hour] Total WorkLoad [Hour]
Theoretical 14 3 42
Practicals/Labs 0 0 0
Self Study and Preparation 14 2 28
Homeworks, Performances 1 20 20
Projects 0 0 0
Field Studies 0 0 0
Midtermexams 1 40 40
Others 0 0 0
Final Exams 1 50 50
Total WorkLoad 180
Total workload/ 30 hr 6
ECTS Credit of the Course 6
26 CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS
PQ1 PQ2 PQ3 PQ4 PQ5 PQ6 PQ7 PQ8 PQ9 PQ10
LO1 4 0 4 4 3 0 0 0 0 0
LO2 0 0 3 4 3 0 0 0 0 0
LO3 4 0 3 4 3 0 0 0 0 0
LO: Learning Objectives PQ: Program Qualifications
Contribution Level: 1 Very Low 2 Low 3 Medium 4 High 5 Very High
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