1 | Course Title: | CYCLIC VOLTAMMETRY |
2 | Course Code: | KIM5016 |
3 | Type of Course: | Optional |
4 | Level of Course: | Second Cycle |
5 | Year of Study: | 1 |
6 | Semester: | 2 |
7 | ECTS Credits Allocated: | 6 |
8 | Theoretical (hour/week): | 3 |
9 | Practice (hour/week) : | 0 |
10 | Laboratory (hour/week) : | 0 |
11 | Prerequisites: | None |
12 | Recommended optional programme components: | None |
13 | Language: | Turkish |
14 | Mode of Delivery: | Face to face |
15 | Course Coordinator: | Prof. Dr. MEHMET HALUK TÜRKDEMİR |
16 | Course Lecturers: | Yok |
17 | Contactinformation of the Course Coordinator: |
Tlf: 2941741 e-mail: hturkdemir@uludag.edu.tr |
18 | Website: | |
19 | Objective of the Course: | This course is planned for to learn of knowledge about cyclic voltammetry basic knowledge and electrochemical characterization of various substances, and especially planned for graduate students from outside of the Electrochemistry. |
20 | Contribution of the Course to Professional Development |
21 | Learning Outcomes: |
|
22 | Course Content: |
Week | Theoretical | Practical |
1 | Cyclic voltammetry definition and usage, basic information of potentiostat | |
2 | Three-electrode cell voltammetry, the components, the electrode-solution interface, double layer structure, junction potential. | |
3 | The working electrodes (WE), variation and selection, selection criteria, GCE and Pt electrode | |
4 | Mercury working electrodes, working surface area | |
5 | Voltammetric reference electrode, types and characteristics | |
6 | Auxiliary electrode and the required properties, IR drop, IR Compensation | |
7 | Supporting electrolyte, specifications, oxygen removal, | |
8 | Establishment of potential screening programs, scanning speed, potential limits, number of cycles | |
9 | Peak potential, peak current and measurements, Randles-Sevcik equation | |
10 | General reminders, description of unifying concepts and Midterm | |
11 | Reversibility, semi-reversibility, irreversibility in cyclic voltammetry curves. | |
12 | Electron transfer mechanisms, gradual electron transfer steps and be monitored on voltammograms | |
13 | Examination of EC, CE, ECE and mechanisms, effects on voltammograms. | |
14 | Cyclic voltammetry in an anhydrous conditions, solvents, supporting electrolyte, reference electrodes, pseudo-reference electrode for non-aqueous solutions. |
23 | Textbooks, References and/or Other Materials: |
1. Techniques and Mechanisms in Electrochemistry, P.A. Christensenand A. Hamnett, Kluwer Acad. Pub.1994 2. Fundamentals of Electrochemistry, V. S. Bagotsky, WILEY 2006 3. Electrochemistry, Principles, Methods, and Applications, C.M.A. Brett, A.M.O. Brett, Oxford 1993 4. Analytical Electrochemistry, J. Wang, WILEY 2001 |
24 | Assesment |
TERM LEARNING ACTIVITIES | NUMBER | PERCENT |
Midterm Exam | 1 | 30 |
Quiz | 0 | 0 |
Homeworks, Performances | 1 | 10 |
Final Exam | 1 | 60 |
Total | 3 | 100 |
Contribution of Term (Year) Learning Activities to Success Grade | 40 | |
Contribution of Final Exam to Success Grade | 60 | |
Total | 100 | |
Measurement and Evaluation Techniques Used in the Course | ||
Information | The weights of the activities can vary within regulations. |
25 | ECTS / WORK LOAD TABLE |
Activites | NUMBER | TIME [Hour] | Total WorkLoad [Hour] |
Theoretical | 14 | 3 | 42 |
Practicals/Labs | 0 | 0 | 0 |
Self Study and Preparation | 14 | 2 | 28 |
Homeworks, Performances | 1 | 20 | 20 |
Projects | 0 | 0 | 0 |
Field Studies | 0 | 0 | 0 |
Midtermexams | 1 | 40 | 40 |
Others | 0 | 0 | 0 |
Final Exams | 1 | 50 | 50 |
Total WorkLoad | 180 | ||
Total workload/ 30 hr | 6 | ||
ECTS Credit of the Course | 6 |
26 | CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS | ||||||||||||||||||||||||||||||||||||||||||||
|
LO: Learning Objectives | PQ: Program Qualifications |
Contribution Level: | 1 Very Low | 2 Low | 3 Medium | 4 High | 5 Very High |