COURSE SYLLABUS
STRUCTURE DETERMINATION BY NMR SPECTROSCOPY
| 1 |
Course Title: |
STRUCTURE DETERMINATION BY NMR SPECTROSCOPY |
| 2 |
Course Code: |
KIM5048 |
| 3 |
Type of Course: |
Optional |
| 4 |
Level of Course: |
Third Cycle |
| 5 |
Year of Study: |
1 |
| 6 |
Semester: |
2 |
| 7 |
ECTS Credits Allocated: |
6 |
| 8 |
Theoretical (hour/week): |
3 |
| 9 |
Practice (hour/week) : |
0 |
| 10 |
Laboratory (hour/week) : |
0 |
| 11 |
Prerequisites: |
None |
| 12 |
Recommended optional programme components: |
None |
| 13 |
Language: |
Turkish |
| 14 |
Mode of Delivery: |
Face to face |
| 15 |
Course Coordinator: |
Prof. Dr. GANİ KOZA |
| 16 |
Course Lecturers: |
Prof. Dr. Necdet COŞKUN |
| 17 |
Contactinformation of the Course Coordinator: |
ganikoza@uludag.edu.tr
+90 224 27 55 083
Uludağ Üniversitesi, Fen-Edebiyat Fakültesi, Kimya Bölümü, 16059 Görükle / BURSA, TÜRKİYE
|
| 18 |
Website: |
|
| 19 |
Objective of the Course: |
The aim of this course is to teach students determination of structure of organic molecules with Nucleer Magnetic Resonance Spectroscopy |
| 20 |
Contribution of the Course to Professional Development |
Can characterize the structures of organic molecules by learning NMR. |
| 21 |
Learning Outcomes: |
| 1 |
The student will learn the behavior of atomic nuclei in the magnetic field and fundamentals of NMR spectroscopy;
|
| 2 |
The student will learn 1H NMR spectrum and chemical shift values of protons;
|
| 3 |
The student will learn magnetic and diamagnetic anisotropy;
|
| 4 |
The student will learn spin-spin interaction;
|
| 5 |
The student will learn 13C NMR spectroscopy and determination of carbons by DEPT method;
|
| 6 |
The student will learn advanced techniques such as COSY and HETCOR spectra in NMR spectroscopy;
|
| 7 |
The student will learn the determination of structure of organic molecules by NMR spectroscopy;
|
|
| Week |
Theoretical |
Practical |
| 1 |
Magnetic properties of the atomic nucleus and NMR active nuclei |
|
| 2 |
Behavior of atomic nuclei in magnetic field and fundamentals of NMR spectroscopy |
|
| 3 |
Introduction to 1H NMR spectroscopy |
|
| 4 |
Chemical shift |
|
| 5 |
Chemical shift values of some functional groups |
|
| 6 |
Magnetic and diamagnetic anisotropy |
|
| 7 |
Spin-spin interaction |
|
| 8 |
Midterm Exam |
|
| 9 |
13C NMR spectroscopy |
|
| 10 |
Determination of carbon signals by DEPT method |
|
| 11 |
Determination of structure by COSY NMR spectrum |
|
| 12 |
Determination of structure by HETCOR NMR spectrum |
|
| 13 |
Determination of structure of unknown molecules by NMR spectroscopy |
|
| 14 |
Determination of structure of unknown molecules by NMR spectroscopy |
|
| 23 |
Textbooks, References and/or Other Materials: |
Nükleer Manyetik Rezonans Spektroskopisi. Prof. Dr. Metin Balcı, Eğitim Yayınevi |
| 24 |
Assesment |
|
| TERM LEARNING ACTIVITIES |
NUMBER |
PERCENT |
| Midterm Exam |
1 |
20 |
| Quiz |
0 |
0 |
| Homeworks, Performances |
1 |
20 |
| Final Exam |
1 |
60 |
| Total |
3 |
100 |
| Contribution of Term (Year) Learning Activities to Success Grade |
40 |
| Contribution of Final Exam to Success Grade |
60 |
| Total |
100 |
| Measurement and Evaluation Techniques Used in the Course |
Homeworks and written exams |
| Information |
|
| 25 |
|
ECTS / WORK LOAD TABLE |
| Activites |
NUMBER |
TIME [Hour] |
Total WorkLoad [Hour] |
| Theoretical |
14 |
3 |
42 |
| Practicals/Labs |
0 |
0 |
0 |
| Self Study and Preparation |
14 |
3 |
42 |
| Homeworks, Performances |
1 |
8 |
48 |
| Projects |
0 |
0 |
0 |
| Field Studies |
0 |
0 |
0 |
| Midtermexams |
1 |
23 |
23 |
| Others |
0 |
0 |
0 |
| Final Exams |
1 |
25 |
25 |
| Total WorkLoad |
|
|
180 |
| Total workload/ 30 hr |
|
|
6 |
| ECTS Credit of the Course |
|
|
6 |
| 26 |
CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS |
|
PQ1
|
PQ2
|
PQ3
|
PQ4
|
PQ5
|
PQ6
|
PQ7
|
PQ8
|
PQ9
|
PQ10
|
|
LO1
|
3
|
4
|
5
|
4
|
5
|
3
|
4
|
4
|
4
|
5
|
|
LO2
|
4
|
2
|
4
|
4
|
4
|
5
|
3
|
4
|
5
|
4
|
|
LO3
|
4
|
5
|
3
|
5
|
4
|
3
|
5
|
4
|
4
|
5
|
|
LO4
|
4
|
5
|
3
|
2
|
4
|
4
|
5
|
5
|
4
|
3
|
|
LO5
|
5
|
4
|
4
|
3
|
4
|
3
|
4
|
4
|
4
|
5
|
|
LO6
|
4
|
4
|
5
|
5
|
3
|
3
|
2
|
2
|
4
|
5
|
|
LO7
|
4
|
5
|
4
|
4
|
5
|
5
|
3
|
4
|
4
|
3
|
|
| LO: Learning Objectives |
PQ: Program Qualifications |
| Contribution Level: |
1 Very Low |
2 Low |
3 Medium |
4 High |
5 Very High |
