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COURSE SYLLABUS
MASS SPECTROMETRY IN ORGANIC CHEMISTRY
1 Course Title: MASS SPECTROMETRY IN ORGANIC CHEMISTRY
2 Course Code: KIM4052
3 Type of Course: Optional
4 Level of Course: First Cycle
5 Year of Study: 4
6 Semester: 8
7 ECTS Credits Allocated: 5
8 Theoretical (hour/week): 3
9 Practice (hour/week) : 0
10 Laboratory (hour/week) : 0
11 Prerequisites: None However, it is strongly recommended that students should have read Organic Chemistry I and Organic Chemistry II.
12 Recommended optional programme components: None
13 Language: Turkish
14 Mode of Delivery: Face to face
15 Course Coordinator: Doç.Dr. NEVİN ARIKAN ÖLMEZ
16 Course Lecturers: Prof. Dr. Necdet COŞKUN
Prof. Dr. Mustafa TAVASLI
17 Contactinformation of the Course Coordinator: narikan@uludag.edu.tr
+90 224 29 41731
Uludag University
Faculty of Sciences and Arts
Department of Chemistry
16059 Gorukle / BURSA
18 Website:
19 Objective of the Course: The aim of this course is to explain the basic principles and differences of the most used modern mass spectrometry techniques and to determine the structures of organic compounds using the mass spectrum
20 Contribution of the Course to Professional Development To learn the basic principles and differences of the most used modern mass spectrometry techniques.
21 Learning Outcomes:
1 Knowing the basic aspects of mass spectrometry;
2 Learning the working principle of mass spectrometer.;
3 Knowing the modern mass spectrometry techniques and application areas;
4 Learning the determination of structures of organic compounds with Mass spectrum;
22 Course Content:
Week Theoretical Practical
1 Introduction, Principles Diagram of a Mass Spectrometer, History, Application areas of mass spectrometry.
2 Calculation of molecular masses, mass units.
3 Mass Spectrometer
4 Ionization techniques; Formation and Fragmentation of Ions.
5 Mass Analysers ; Quadrupole Analysers Ion Trap Analysers ,The Electrostatic Trap or ‘Orbitrap’, Time-of-Flight Analysers , Magnetic and Electromagnetic Analysers, Ion Cyclotron Resonance and Fourier Transform Mass Spectrometry , Hybrid Instruments.
6 Detectors and Computers
7 Mass spectrum and peak types: Molecular ion peak, Isotopic peaks, Peaks of molecular fragments, ion-molecule peaks, Double charged ion peaks, Semi-stable peaks.
8 Problem solving
9 Types of molecular fragmentation
10 Molecular fragmentation according to functional group
11 Mass spectrum, structure determination
12 Mass spectrum, structure determination
13 Other mass spectrometry techniques
14 Problem Solving
23 Textbooks, References and/or Other Materials: Edmond De Hoffmann & Vincent Stroobant, Mass Spectrometry: Principles and Applications,, 3rd ed., John Wiley, 2007
-Jürgen H Gross, Mass Spectrometry: A Textbook, 2nd ed., Springer-Verlag, 2011.
-J.Throck Watson & O. David Sparkman, Introduction to Mass Spectrometry: Instrumentation, Applications, and Strategies for Data Interpretation, 4th ed., John Wiley, 2007.
-Ender Erdik, Organik Kimyada Spektroskopik Yöntemler
24 Assesment
TERM LEARNING ACTIVITIES NUMBER PERCENT
Midterm Exam 1 40
Quiz 0 0
Homeworks, Performances 0 0
Final Exam 1 60
Total 2 100
Contribution of Term (Year) Learning Activities to Success Grade 40
Contribution of Final Exam to Success Grade 60
Total 100
Measurement and Evaluation Techniques Used in the Course It is evaluated by midterm exam, and final exam, which consists of classical questions, and homework.
Information
25 ECTS / WORK LOAD TABLE
Activites NUMBER TIME [Hour] Total WorkLoad [Hour]
Theoretical 14 3 42
Practicals/Labs 0 0 0
Self Study and Preparation 13 1 13
Homeworks, Performances 0 0 0
Projects 0 0 0
Field Studies 0 0 0
Midtermexams 1 48 48
Others 0 0 0
Final Exams 1 48 48
Total WorkLoad 151
Total workload/ 30 hr 5,03
ECTS Credit of the Course 5
26 CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS
PQ1 PQ2 PQ3 PQ4 PQ5 PQ6 PQ7 PQ8 PQ9 PQ10 PQ11 PQ12 PQ13
LO1 0 5 0 5 0 0 0 0 0 0 0 0 0
LO2 0 5 0 5 0 0 0 0 0 0 0 0 0
LO3 0 5 0 5 0 0 0 0 0 0 0 0 0
LO4 0 5 0 5 0 0 0 0 0 0 0 0 0
LO: Learning Objectives PQ: Program Qualifications
Contribution Level: 1 Very Low 2 Low 3 Medium 4 High 5 Very High
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