1	Course Title:	NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY IN ORGANIC STRUCTURE IDENTIFICATION
2	Course Code:	KIM6014
3	Type of Course:	Optional
4	Level of Course:	Third Cycle
5	Year of Study:	1
6	Semester:	2
7	ECTS Credits Allocated:	6
8	Theoretical (hour/week):	3
9	Practice (hour/week) :	0
10	Laboratory (hour/week) :	0
11	Prerequisites:
12	Recommended optional programme components:	None
13	Language:	Turkish
14	Mode of Delivery:	Face to face
15	Course Coordinator:	Prof. Dr. NECDET COŞKUN
16	Course Lecturers:	Prof. Dr. GANİ KOZA
17	Contactinformation of the Course Coordinator:	Prof. Dr. Necdet Coşkun Kimya Bölümü
18	Website:
19	Objective of the Course:	The aim of the course is to enhance theoretical knowledge and skills of students (deal with organic synthesis) in one-and two-dimensional NMR techniques so they can use these skills in structural interpretations.
20	Contribution of the Course to Professional Development	To be able to solve organic structural issues by 1 and 2D NMR technics

21

Learning Outcomes:

1 Inreasing of theoretical info and skills about NMR structure identification; 2 Using the NMR technique in structure identification with advanced level and acquiring the construe ability of NMR spectrum; 3 Learning in advanced level about of applications of the certain techniques that use in organic compound characterizations;

22	Course Content:

Week	Theoretical	Practical
1	Basic approaches in structure elucidation - Nuclear Magnetic Resonance - Infrared Spectroscopy - Electronic Spectroscopy - Mass Spectroscopy their applications area
2	- Electromagnetic spectrum - Detection of molecular weight and molecular formula
3	- Structural isomers and stereoisomers
4	- Magnetic properties of nucleus - Chemical shift - Expansion and relaxation - Coupling constants
5	- Spectrometers and samples - Signal optimization - Dynamic effects, spectra of solid samples
6	- Factors causing proton chemical shifts
7	- Saturated and unsaturated aliphatics, chemical shifts of protons bonded to nitrogen and oxygen
8	- Factors causing carbon chemical shifts
9	- Saturated and unsaturated aliphatics, carbonyl groups, interpretation of carbon spectra, structure identification
10	- Spectral analysis, spin lattice and spin-spin relaxations - NMR time scale reactions - Multiple resonance - Nuclear Overhauser effect
11	- Spectral data - Multiple pulses and samples - Proton-proton interactions (COSY) spectra interpretation
12	- Total correlation spectroscopy (TOCSY) - Proton-heteronuclear spectra of other compounds, (NOESY, HETCOR) interpretation
13	- Total correlation spectroscopy (TOCSY) - Proton-heteronuclear spectra of other compounds, (NOESY, HETCOR) interpretation
14	- carbon-carbon correlations - INADEQUATE experiments and applications

23	Textbooks, References and/or Other Materials:	Organik Structural Spectroscopy, Josef B. Lambert, herbert F. Shurvell, David A. Lightner, R. Graham Cooks
24	Assesment

TERM LEARNING ACTIVITIES	NUMBER	PERCENT
Midterm Exam	0	0
Quiz	0	0
Homeworks, Performances	1	40
Final Exam	1	60
Total	2	100
Contribution of Term (Year) Learning Activities to Success Grade		40
Contribution of Final Exam to Success Grade		60
Total		100
Measurement and Evaluation Techniques Used in the Course	relative evaluation
Information

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ECTS / WORK LOAD TABLE

Activites	NUMBER	TIME [Hour]	Total WorkLoad [Hour]
Theoretical	14	3	42
Practicals/Labs	0	0	0
Self Study and Preparation	14	1	14
Homeworks, Performances	1	70	70
Projects	0	0	0
Field Studies	0	0	0
Midtermexams	0	0	0
Others	0	0	0
Final Exams	1	50	50
Total WorkLoad			176
Total workload/ 30 hr			5,87
ECTS Credit of the Course			6

26	CONTRIBUTION OF LEARNING OUTCOMES TO PROGRAMME QUALIFICATIONS
PQ1 PQ2 PQ3 PQ4 PQ5 PQ6 PQ7 PQ8 PQ9 PQ10 LO1 4 0 3 0 0 0 0 0 0 0 LO2 0 0 0 0 0 0 0 0 0 0 LO3 0 0 0 0 0 0 0 0 0 0

LO: Learning Objectives

PQ: Program Qualifications

Contribution Level:

1 Very Low

2 Low

3 Medium

4 High

5 Very High